American Society for Testing and Materials (ASTM). Current edition approved Sept. 1, 2005. Published September 2005. Originally approved in 1979. Last previous edition approved in 1999 as D 3872 – 86 (1999). 3 p. This test method covers the quantitative determination of ferrous oxide (FeO) by oxidation of ferrous iron (Fe++) in an acid solution to the ferric state (Fe+++) and titration with potassium dichromate using diphenylamine as the indicator.