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Schubert U., Hüsing N., Laine R. (eds.) Materials Syntheses: A Practical Guide

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Schubert U., Hüsing N., Laine R. (eds.) Materials Syntheses: A Practical Guide
Springer-Verlag / Wien, 2008. VII, 228 p. — ISBN 978-3-211-75124-4 (SpringerWienNewYork).
First book on detailed materials synthesis protocols
Presents unambiguous descriptions of hardware, specific synthetic procedures and characterization methods
Serves as a helpful manual for laboratory courses in materials chemistry
Materials syntheses are generally more complex than syntheses of inorganic or organic compounds and specific characterization methods play a more important role. Materials synthesis protocols often suffer from unclarities, irreproducibility, lack in detail and lack in standards. The need to change this situation is the main motivation for this book. It collects a number of detailed protocols, ranging from organic polymers to carbonaceous and ceramic materials, from gels to porous and layered materials and from powders and nanoparticles to films. Preparation methods include intercalation and flux methods, sol-gel processing, templating methods for porous materials, sonochemistry or spray pyrolysis.
Each contribution provides detailed and unambiguous descriptions of the hardware, specific characteristics of the procedure, scope of applicability as well as methods that unequivocally identify and characterize the material and allow checking whether the synthesis was successful.
Content Level » Research
Keywords » Inorganic Chemistry - Materials - Materials Chemistry - Materials Synthesis -Practical Guide - Synthesis
Related subjects » Inorganic Chemistry - Materials - Nanotechnology.
Contents
Preface
List of Contributors
Controlling Size and Morphology of Zeolite L
Large Zeolite L Crystals
Medium-sized Disc-shaped Zeolite L Crystals
Nano-sized Zeolite L Crystals
Medium-sized Cylindrical-shaped Zeolite L Crystals
Zeolite A and ZK-4
Zeolite A Crystals
ZK-4 Crystals
Nano-sized Zeolite A Crystals (Fig. 4)
Mesostructured Silica Thin Films
Preparation of the Coating Sol
Film Deposition
Post Treatment
Organically Modified Monolithic Silica Aerogels
Preparation of 3-Methacryloxypropyl-substituted Silica Aerogel
Preparation of 2-Aminoethyl-3-aminopropyl-substituted Silica Aerogel
Porous Silica Gel by Acid Leaching of Metakaolin
Preparation of Metakaolins
Preparation of the Acid-activated Solids
Zirconia-Pillared Clays
Preparation of Zr-pillared Clays Using Zirconyl Chloride as Precursor
Preparation of Zr-pillared Clays Using Zirconium Acetate as Precursor
Montmorillonites with Mixed Aluminum-Lanthanide Oxide Pillars
Preparation of the Pillaring Agent
Pillaring Process
Birnessite-type Manganese Oxide by Redox Precipitation
Redox Precipitation
Hydrothermal Treatment
Templated Carbon from Pyrolysis of Pyrene in Pillared Clay Matrices
Preparation of Pillared Clay
Loading of the Pillared Clay with Organic Compounds
Pyrolysis, and Removal of the Inorganic Matrix
Fiberous Carbon from Sepiolite Clay and Propylene
Preparation of Propylene-loaded Sepiolite
Pyrolysis and Dissolution of the Propylene-loaded Sepiolite
Aerosol Spray Synthesis of Porous Molybdenum Sulfide Powder
Preparation of Low-porosity MoS
Preparation of Porous MoS
Sonochemically Prepared Molybdenum Sulfide
Preparation in Glove Box
Reaction in Fume Hood
Product Isolation
Doped Manganites
Preparation of La0.5Ba0.5MnO
Preparation of La0.5Sr0.5MnO
Lithium Manganese Oxide Prepared by Flux Methods
Growth of LiMn2O4 Spinel Single Crystals in a LiCl-Mn(NO3)2 Flux
Growth of LiMn2O4 Spinel Single Crystals in a LiCl-MnCl2 Flux
Nanoscale Magnesium Oxide
Nanostructured Pt-doped Tin Oxide Films
Preparation of Tetra(tert-butoxy)tin
Preparation of the Sol for Coating
Film Deposition and Annealing
Organically Functionalized Silica Nanoparticles
Synthesis of SiO2 Nanoparticles
Preparation of 2-[4-(Chloromethyl)phenyl]ethyltriethoxysilane
Functionalization of the Silica Particles
Copper Nanoparticles in Silica
Sol-Gel Processing of Alkoxysilyl-substituted Metal Complexes
Oxidation
Reduction
Copper Nanocrystals
Assembly of TOPO-Capped Silver Nanoparticles to Multilayered Films
Preparation of Silver Hydrosols
Transfer of the Silver Nanoparticle Sol into Organic Solvents
Multilayered Film Synthesis
Colloidal Dispersion of Gold Nanoparticles
Preparation of HAuCl4ǜ3H2O
Preparation of Gold Nanoparticles Colloidal Suspension
One-dimensional Nanorods and Nanowires
Preparation of Gold Seeds
Preparation of Growth Solution
Preparation of Gold Nanorods and Wires
Monolithic Tin-doped Silica Glass
Sol Preparation
Sol-Gel Transition and Drying
Thermal Treatment and Glass Formation
Sintering Process A
Sintering Process B
Octaphenyloctasilsesquioxane and Polyphenylsilsesquioxane for Nanocomposites
Synthesis of Phenyltriethoxysilane (PTES)
Synthesis of OPS and its Polymeric Analog PPS from PTES
Polysilsesquicarbodiimide Xerogels
Polyaniline – A Conducting Polymer
Preparation of Polyaniline Hydrochloride
Preparation of Polyaniline Base
Allyl- and Hydroxytelechelic Poly(isobutylenes)
Syntheses of Allyl-telechelic PIB (1)
Syntheses of Hydroxyl-telechelic PIBs (2)
Symmetrically and Unsymmetrically Substituted Phthalocyanines
Procedure A
Procedure B
Index
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