Springer-Verlag / Wien, 2008. VII, 228 p. — ISBN 978-3-211-75124-4 (SpringerWienNewYork).First book on detailed materials synthesis protocols Presents unambiguous descriptions of hardware, specific synthetic procedures and characterization methods Serves as a helpful manual for laboratory courses in materials chemistry Materials syntheses are generally more complex than syntheses of inorganic or organic compounds and specific characterization methods play a more important role. Materials synthesis protocols often suffer from unclarities, irreproducibility, lack in detail and lack in standards. The need to change this situation is the main motivation for this book. It collects a number of detailed protocols, ranging from organic polymers to carbonaceous and ceramic materials, from gels to porous and layered materials and from powders and nanoparticles to films. Preparation methods include intercalation and flux methods, sol-gel processing, templating methods for porous materials, sonochemistry or spray pyrolysis. Each contribution provides detailed and unambiguous descriptions of the hardware, specific characteristics of the procedure, scope of applicability as well as methods that unequivocally identify and characterize the material and allow checking whether the synthesis was successful.Content Level » Research Keywords » Inorganic Chemistry - Materials - Materials Chemistry - Materials Synthesis -Practical Guide - Synthesis Related subjects » Inorganic Chemistry - Materials - Nanotechnology.ContentsPreface List of ContributorsControlling Size and Morphology of Zeolite LLarge Zeolite L Crystals Medium-sized Disc-shaped Zeolite L Crystals Nano-sized Zeolite L Crystals Medium-sized Cylindrical-shaped Zeolite L CrystalsZeolite A and ZK-4Zeolite A Crystals ZK-4 Crystals Nano-sized Zeolite A Crystals (Fig. 4)Mesostructured Silica Thin FilmsPreparation of the Coating Sol Film Deposition Post TreatmentOrganically Modified Monolithic Silica AerogelsPreparation of 3-Methacryloxypropyl-substituted Silica Aerogel Preparation of 2-Aminoethyl-3-aminopropyl-substituted Silica AerogelPorous Silica Gel by Acid Leaching of MetakaolinPreparation of Metakaolins Preparation of the Acid-activated SolidsZirconia-Pillared ClaysPreparation of Zr-pillared Clays Using Zirconyl Chloride as Precursor Preparation of Zr-pillared Clays Using Zirconium Acetate as PrecursorMontmorillonites with Mixed Aluminum-Lanthanide Oxide PillarsPreparation of the Pillaring Agent Pillaring ProcessBirnessite-type Manganese Oxide by Redox PrecipitationRedox Precipitation Hydrothermal TreatmentTemplated Carbon from Pyrolysis of Pyrene in Pillared Clay MatricesPreparation of Pillared Clay Loading of the Pillared Clay with Organic Compounds Pyrolysis, and Removal of the Inorganic MatrixFiberous Carbon from Sepiolite Clay and PropylenePreparation of Propylene-loaded Sepiolite Pyrolysis and Dissolution of the Propylene-loaded SepioliteAerosol Spray Synthesis of Porous Molybdenum Sulfide PowderPreparation of Low-porosity MoS Preparation of Porous MoSSonochemically Prepared Molybdenum SulfidePreparation in Glove Box Reaction in Fume Hood Product IsolationDoped ManganitesPreparation of La0.5Ba0.5MnO Preparation of La0.5Sr0.5MnOLithium Manganese Oxide Prepared by Flux MethodsGrowth of LiMn2O4 Spinel Single Crystals in a LiCl-Mn(NO3)2 Flux Growth of LiMn2O4 Spinel Single Crystals in a LiCl-MnCl2 FluxNanoscale Magnesium OxideNanostructured Pt-doped Tin Oxide FilmsPreparation of Tetra(tert-butoxy)tin Preparation of the Sol for Coating Film Deposition and AnnealingOrganically Functionalized Silica NanoparticlesSynthesis of SiO2 Nanoparticles Preparation of 2-[4-(Chloromethyl)phenyl]ethyltriethoxysilane Functionalization of the Silica ParticlesCopper Nanoparticles in SilicaSol-Gel Processing of Alkoxysilyl-substituted Metal Complexes Oxidation ReductionCopper NanocrystalsAssembly of TOPO-Capped Silver Nanoparticles to Multilayered FilmsPreparation of Silver Hydrosols Transfer of the Silver Nanoparticle Sol into Organic Solvents Multilayered Film SynthesisColloidal Dispersion of Gold NanoparticlesPreparation of HAuCl4ǜ3H2O Preparation of Gold Nanoparticles Colloidal SuspensionOne-dimensional Nanorods and NanowiresPreparation of Gold Seeds Preparation of Growth Solution Preparation of Gold Nanorods and WiresMonolithic Tin-doped Silica GlassSol Preparation Sol-Gel Transition and Drying Thermal Treatment and Glass Formation Sintering Process A Sintering Process BOctaphenyloctasilsesquioxane and Polyphenylsilsesquioxane for NanocompositesSynthesis of Phenyltriethoxysilane (PTES) Synthesis of OPS and its Polymeric Analog PPS from PTESPolysilsesquicarbodiimide XerogelsPolyaniline – A Conducting PolymerPreparation of Polyaniline Hydrochloride Preparation of Polyaniline BaseAllyl- and Hydroxytelechelic Poly(isobutylenes)Syntheses of Allyl-telechelic PIB (1) Syntheses of Hydroxyl-telechelic PIBs (2)Symmetrically and Unsymmetrically Substituted PhthalocyaninesProcedure A Procedure BIndex
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